1、 File .MS03Data2017112820171128WSY4922-001-2.D Tgt Mass (CHM):Injection Date : 28 Nov 17 8:05 pm +0800 Seq. Line : 135Sample Name : WSY4922-001-2 Location : P2-F-01Acq. Operator : SYSTEM Inj : 1Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:LCMS03Data20171128201711281-POS-3MIN(1.2M
2、L).MAnalysis Method : D:LCMS03Data20171128201711281-POS-3MIN(1.2ML).MCatalog No : HY-14802C Batch#27600Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.2ml/minColumn :Poroshell 120 EC-C18, 3.0*50mm,2.7um A-RP-170Oven Temperature : 45Cmin0
3、0.5 1 1.5 2 2.5mAU010002000DAD1 A, Sig=214,4 Ref=off1.3741.4251.4851.9622.0062.1472.836min0 0.5 1 1.5 2 2.5mAU05001000DAD1 B, Sig=254,4 Ref=off1.9532.0062.0552.146min0 0.5 1 1.5 2 2.5mV0250500ELS1 A, ELSD Signal2.080min0 0.5 1 1.5 2 2.50200000040000006000000MSD1 TIC, MS File ES-API, Pos, Scan, Frag:
4、 702.0482.895min0 0.5 1 1.5 2 2.5-0.1-0.0500.05Ion 1, MSD1 1,Target Mass 0 +H Positive, EIC=0.7:1.7Integration Results for DAD1 A, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.37 0.01 1.95 0.00 0.06 4761.43 0.01 0.34 0.01 0.01 5891.48 0.01 1.47 0.08 0.04 7021.96 0.01 6.18 10.7
5、5 0.17 2332.01 0.01 2558.38 3468.26 72.32 3092.15 0.12 963.84 131.53 27.25 2432.84 0.02 5.19 0.13 0.15 338Integration Results for DAD1 B, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.95 0.01 1.63 -0.00 0.12 2332.01 0.01 920.98 1427.57 65.46 3092.05 0.01 1.00 0.82 0.07 3092.15
6、0.12 483.28 65.18 34.35 243Integration Results for MSD1 TIC, MS FileMS Report from Instrument: LCMS-03LCMS-03 11/30/2017 16:11:11 ZLJ_587 Page 1 of 4RetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|2.05 0.06 27856298.00 7374947.00 72.27 3092.90 0.07 10689955.00 2533688.00 27.73 338MS Report from Ins
7、trument: LCMS-03LCMS-03 11/30/2017 16:11:11 ZLJ_587 Page 2 of 4Ret. Time: 2.05 m/z100 200 300 400 500 600 700 800 90002000004000006000008000001E6ES-API Positive401.1311.1310.1189.6309.1Ret. Time: 2.90m/z100 200 300 400 500 600 700 800 900050000100000150000200000250000300000350000400000450000ES-API Positive430.9361.3105.1 339.4360.3338.4MS Report from Instrument: LCMS-03LCMS-03 11/30/2017 16:11:11 ZLJ_587 Page 3 of 4* End of Report *MS Report from Instrument: LCMS-03LCMS-03 11/30/2017 16:11:11 ZLJ_587 Page 4 of 4
