1、 File .1-1 2018-02-01 15-18-45CPK2018-201-07938.D Tgt Mass (CHM): Injection Date : 1 Feb 18 5:38 pm +0800 Seq. Line : 28Sample Name : CPK2018-201-07938 Location : P2-C-04Acq. Operator : HCL_771 Inj : 1Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:chem321DATA2018020120180201-1 2018
2、-02-01 15-18-451-POS-3MIN-1.MAnalysis Method : D:CHEM321DATA2018020120180201-1 2018-02-01 15-18-451-POS-3MIN-1.MCatalog No : HY-14460 Batch#07938 A-RP-189Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm
3、,3.5um A-RP-186Oven Temperature : 45Cmin0.5 1 1.5 2 2.5mAU050010001500DAD1 B, Sig=214,4 Ref=off 0.3251.6811.7911.9292.165min0.5 1 1.5 2 2.5mAU0250500750DAD1 C, Sig=254,4 Ref=off 1.0492.165min0.5 1 1.5 2 2.5050000100000150000200000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 702.196min0.5 1 1.5 2 2.501
4、0000200003000040000Ion 693.9, MSD1 693.9,Target Mass 692.9 +H Positive, EIC=693.6:694.6 2.197Integration Results for DAD1 B, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|0.33 0.03 3.91 2.48 0.13 ND1.68 0.05 0.94 0.77 0.03 ND1.79 0.22 0.90 -0.14 0.03 ND1.93 0.06 3.64 1.39 0.12 ND
5、2.16 0.03 2921.04 1907.52 99.68 693Integration Results for DAD1 C, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.05 0.03 0.33 0.30 0.02 ND2.16 0.03 1800.97 1199.50 99.98 693Integration Results for MSD1 TIC, MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|2.20 0.05 68375
6、2.94 224015.41 100.00 693MS Report from Instrument: LCMS-02LCMS-02 2/2/2018 10:46:41 XLH_854 Page 1 of 2Ret. Time: 2.20 m/z200 300 400 500 600 700 800 900050001000015000200002500030000ES-API Positive159.0716.2 695.2694.3 347.1693.2MS Report from Instrument: LCMS-02LCMS-02 2/2/2018 10:46:41 XLH_854 Page 2 of 2
