1、 File .ta2017112020171120-1BIZ2017-N20-WYQ2.D Tgt Mass (CHM):Injection Date : 20 Nov 17 5:13 pm +0800 Seq. Line : 99Sample Name : BIZ2017-N20-WYQ2 Location : P2-A-05Acq. Operator : SYSTEM Inj : 1Spec. Reported : MS Integration Inj Volume : 0.5 ulAcq. Method : D:LCMS03Data2017112020171120-11-POS-3MIN
2、(1.2ML).MAnalysis Method : D:LCMS03Data2017112020171120-11-POS-3MIN(1.2ML).MCatalog No : HY-16687A Batch#27335Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.2ml/minColumn :SunFire C18, 4.6*50mm,2.7um A-RP-170Oven Temperature : 45Cmin0 0.
3、5 1 1.5 2 2.5mAU0500DAD1 A, Sig=214,4 Ref=off1.2681.2951.4081.4571.4691.5291.6051.6451.7081.927min0 0.5 1 1.5 2 2.5mAU050100DAD1 B, Sig=254,4 Ref=off1.2681.2951.4091.4751.6061.6211.9272.096min0 0.5 1 1.5 2 2.5mV20ELS1 A, ELSD Signal1.374min0 0.5 1 1.5 2 2.505000001000000MSD1 TIC, MS File ES-API, Pos
4、, Scan, Frag: 701.342min0 0.5 1 1.5 2 2.50200400600Ion 293, MSD1 293,Target Mass 292 +H Positive, EIC=292.7:293.7Integration Results for DAD1 A, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.27 0.01 1.41 2.56 0.10 2211.29 0.02 1382.08 1199.24 99.35 2211.41 0.02 0.11 0.12 0.01 2
5、211.46 0.02 0.20 0.22 0.01 2211.47 0.01 0.10 0.05 0.01 2211.53 0.01 0.16 0.02 0.01 2211.61 0.01 0.44 0.83 0.03 2211.64 0.01 0.26 0.30 0.02 2211.71 0.01 0.26 0.37 0.02 2331.93 0.01 6.13 10.19 0.44 321Integration Results for DAD1 B, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.2
6、7 0.01 0.24 0.44 0.14 2211.29 0.02 167.21 145.06 98.18 2211.41 0.01 0.54 0.68 0.32 2211.47 0.01 0.10 0.27 0.06 221MS Report from Instrument: LCMS-03LCMS-03 11/21/2017 9:12:25 SYSTEM Page 1 of 41.61 0.01 0.11 0.17 0.06 2211.62 0.01 0.03 0.06 0.02 2211.93 0.01 1.89 2.88 1.11 3212.10 0.01 0.21 0.08 0.1
7、2 233Integration Results for MSD1 TIC, MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.34 0.07 4633071.50 1186662.75 100.00 221MS Report from Instrument: LCMS-03LCMS-03 11/21/2017 9:12:25 SYSTEM Page 2 of 4Ret. Time: 1.34 m/z100 200 300 400 500 600 700 800 900050000100000150000200000250000ES-API Positive222.1221.1MS Report from Instrument: LCMS-03LCMS-03 11/21/2017 9:12:25 SYSTEM Page 3 of 4* End of Report *MS Report from Instrument: LCMS-03LCMS-03 11/21/2017 9:12:25 SYSTEM Page 4 of 4
