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2、zlt#PtfltlE EEE 2s ffifitryE iEA&i5wffiHBlullf EEt .-.2+ ffifiiE/E pH EH0flilE dHt 35 firfi trJU flHffimEtullE #ffitriffiEE . . 66 ffirttrJZ ,H.ffiEPtUE +EziiltJffiEtE 87 fifttrvu E ffiHHluE EnffiEr*. . 108 ffifii6JA MHlir|IE *ffitr4-fiEq#bl,ffi?If.J1E.t* .-. 12e firttrUE, e|L+rrtulilp. #tEtrpE-sLV,
3、*WitH.t* 16i0 fifri5ilU AN,Wfr!fifr. #tBtr*Mffi-ffip$ffimhjtr.JtH.l* 1811 fifii5Ua t+rJlfrEliltlE ,rrftlttJtH* . 2212 fifiYryz rr/rlfrBtfltlE Hrl4,i.JhlttrE . 2413 fitligyB frH,H.ryElWE +mitfitE 26t4 ffifitrf,z tffiH#E!illlE *EftHX . 2815 fifittJE itffiH#B!illlE ffiffiE . 3316 ffifii6Ja $E_B,FFHIUII
4、E #rFlt . 3717 fitfii5uz ffie.NtuavJffJiltr HEIHffitrH+FxrW.lltYJ6H* .3ei8 fifiirJz *hHk AWff)fl.nft. HEiHffitrH,l*ffi4+H +t+H,htJti*rA 41re fiIfitrW, #kH4Lefur*1il1Jfr. ffiiEHElHffitrtH,+WW.tlJt;/tE.t 4320 fitfiiEita frh.H4be4/rffJiltl ffiiEHEiHffitrtsl*ffi6$H+E$f/ti#E 4421. ,Ifii5UU ffiKH4I,hWffJi
5、lE HEiHffitr IR+WLW.aJTJTH,* . 4622 fifii6vz Witts.kAWJffrillE HEiHffitrHtsffiA+H+Wfr.fitJtigr* 4823 fifittiE ffih*kawfr+rfliJtr ffi&HtriHffitrtF+rfr.w.hJdtq.* . 4s24 &tftY5ya ffie-Htt#+rrfrtrfillfr. ffi?EHEiHffitrEffiffiA+H+Wts-*tlti*t* 5125 fiffitrYZ #e.Hit1.+rJfr1rfl1ft. HElYffitrlH.+WlE.h)h/ttrI
6、A 5326 ffift?tirE ffieH1P-+VrWNfr. HE.tYffitrtsffiffiA+H+tffts-#DbiB* 5s27 ffifiiriE ffih.Xki+rJfrtrilft. HtrtYffitrlF+*.Jt:r s628 ffifittyz #e.Xtt#+rtfrWtr ffi&HElHffitrlF+rfr.W.il)PltEE 582s fiTFiEtlE Wh.Ntt4+rJffJil!ft. ffiWHElHffi,trH,ffiffiA+H+6ENth1*, 6030 fifii5Jz ffie,Xft,+rrffr&lfr ffiiEHEl
7、Hffitrl*+ft)hFA 623i ffifiiyJE +flh.XtL,A1/Jffiiltft. HElYffitrlF+rfr.qkh)E)hH* 6432 fifiiEiE Wx,Htl+rrf.ilt)ft. HElHffitrEtsffiA+HffffthtJtiBE 6533 firttrJz ffieH./,a+rJffrwfr. ffi&HtrlHffitrlil+rfr.wllttttq.* 67z4 fifii5Uu ffie.HN,EVJffiWtJft ffiiEHEiHffitrH,ffifiBA+H+EhtItffi* 6e3b ffifiitirz ffi
8、ts-4LAt/Jffrfilfr HEiHffitr-#ffiffi-ffihJtttErA 7036 fifitrtrE ffie.NiL#+rrffrilfr. HElYffitrH,ffiffi+H+1fiR.*ttti*r 7337 fiIffiEJe ffieE4L+Wr$ilft. ffi&HElHffitr-tffiW,-ffihJt)bEr* 74ifr.EIwwwwwwwwwwwwwwwwwwcJ/r 221-200538 fittji-rrz3e ffifiltiE40 &tfitrJE41 fitfitrtE42 fiIfi?5iE4s firt7airz44 &tTf
9、itriE,45 firtirYE46 trfiirrlz,47 fifitr/Z48 frfiiiE4e ffifitrilz50 ffifit6ilu51 tffitriEs2 ffifii5/E,s3 fifitriE54 fiIfrf5ilE,*4vffi.ffie.Hk a+rr*lfliJft- ffi&HEtHffi,tr H,*ffiA+H+,f+ E ht*ti*txffi &.HL,A ryr ffrfl|tr H E ?H ffi tr H +Wtt Jh)tE y*ffi XNtt A +rt ffrill ft. H EIH ffi tr H ffi ffi A +
10、H + t&fr.ht JriSE .lfi &H-lL#WJfrttilIft .ffiW.HElHffi trlH+vX.qY.+lltXH.tXffie.X4t +WrffrilItr ffiiEEElHffitr EBffi+ +H+l+H.Ff /6iSI*i4 &Ett + +rr WUfr. H EtHffi tr IF-+*.ttFiqe.H4L,dPJffrWft. H rrIHffitr tr/*ffiA+H +Wn WXjBE .fr+ E,H K,# WJ frIJ fll fr ffi iE H tr iH ffi tr H B ffi A + H + + E.hT
11、)Li*IXMfl E.H K,A +,J ffJ frIJ ft. H E iH ffi tr E tsffi A S H + W E.hT )YiE * .ffin hH 4t d +rr ffJ ilt) ft.ffiWH ElHffi tr ts ffi A + H +,f+ H.ht Jbi* W,H.ff et iflU E ffi ltrYffi m W tHffi H rl tlJi)tE.*,H.ffi 6!UIE Afi ft,ffr ffi ffitr ffi+frfr.itttJtEtr,H.ffi HlIftIE HEiHffi tr H,ffiffia+H + WE
12、.hIJbiBE.788082848587899193949698100102104106108wwwwwwwwwwwwwwwwwwcJ/r 221-2005+EItrrTfrill&ffifr?szi4l-H!iaHgrE,*ififilfii:zjt4tE&?Ei/V,4!4iAfifr?X,4EW.gT:&-WF, & H ffi fi fr tK &.ti tft ff) qi # ra effi # e fil H tul aE rt, ffi E A R ffi ffi , w +F H. *+ ffi +.* ui H, ftll E4&nfi + ffi E fi ffi Hi
13、kffi ffifr cJ J 6 0- e 4( ffi fi ir zl &t Is I- i6 17, WtF D.* X + &. * *nE ) tr *L E Ht i5 ffi4t4r5fT&6ffi4nft8. H+iEft,AEBot&UllBrfr9lt-tr&u-t*nrn,i5tE+#eEk:t&fl|l,HTHEfrEFt#FzJW.Wlt)Lf0hffily#1ft&H!EpR,+tmtFfr+Yl.hnffi)it*tu1ffifriJ,lEIH-f&ffi?EzK4LlE& tr E iI B at h.*.*E rF, & ffi 1lll ffi E & H
14、 ifltl flt fA H$ E iy, tr +t f tEtr H in T ir JU ft s; ?+ tr,f+ W H&ulla E.+tlriEi6,H Tffif i5zJ&IrEI- tEiE&UI , fi&fiFtKr.kffi.-H,fttEXP!ttrrA+ kt &UtI .4ffiIEl+ 24 +&illrF Et ,s+ .16i4l,.i.tfin* +hiW.#ffiff H! ilE + ,fHgE f E ffi . tr Fr E ffi)lL -Elfi,41)tI-H! ftit E! t$ifil ,tfi & & UU +n IE.Bl!
15、il*Hffi.$.1Yffifr.frHffiEfrarE,+H+fr.ht)Li#iE#traE,tF+fr)tt*hffititft,+ffifrers+. Erf#,EI9iEFJtrffi&Utli-E,&fltl,Ee&:il#&*:r#*,lEH-rfr,EE!r-tf&ifllrm,EE6E&t+ * ffi &.ifl ll tr E, H H ffi&lLh +fi ea ffi M ly +* h ffi , H tfi. H x trtfl ll E 4 H Ef tr E .4t6lE H E*n% zJt fFzKF ffi tm W|N,#.*E * tE n A
16、+.nlE H B,S fi fi ffi flF zlffi fll n$ri ff EH .#FttF*finEH+fn JtHfifilftflFzJcHfllJ,H. ffi , -Lt& frfiftfiFzjffiiIUn* , f fl i &lfifiFzKHiUff ,W#rlfizK# *WAPPdzKtr&ifltl+,1.,4i&fifiIfifiF2Kffi WJnfr,A*ff.ft&tfiflFuJffiIfitli* ,i& tr fifififlFzjcHifltlifi HHfi&lfiflFzKffiflrlffi,Etlfi&IfifiFzKffifln
17、fi,fi*fiffififlFzjcffiXtrlifi,trt-fifitfffiFzKHilUifi,ffi,11lTFffifi fiFz&ffiiflrlifi,EEEffifilfiflFzjHtfl|lifi,7uHfifififiFzlffiilrjf6,XBrtfiIftfiFzKHru,fi pfl.fiEfifitfiflFzKHzu ifi , +fiffififrftflFzjHtrU nS , AxEfi filfi fiFzJcHflUn# , JLH HX,fX#$A pEA-.1, ,S fi ?4 * W. * Il E trf* #F zl H fltl
18、n6, H,S,& i+ W ffi.W Ffi +&T re *EEH *F ffi . H tr. ffi l9 . r H = . il zl &. E 6 nE . ?Jt fi W. + t t . $t H . Wsttr.ffi,1rfi.EEffi ,El*Lt,Hffi$tntL* l:n*&iiT Et E ,ftlffiH-.7Is . f I ft ,?l*.+. +ffi. ffi*.,+-t. tr+_u. Hff .fl 4 . rr E EE, #.Wtk. ffi :1 + . E n +, M W &.1-r ll# w . ffi i6 . S ffi .
19、 E fr ru . ffi . * tr . iE E* ffi . t|J & .ffiffi,ffi ,frE tt Y .4 ft,fr.lEl# . +ffi . + ffi ffi . + + gr .tr*. + 4 ffi . r i& ff . + ffi E . A s = . - + r* .tfrH,t+,W*.6. ilffi H . 74 8. ffi ft ,s .tq rd *. IrJ I 6 . + ffi & . 8 ffi . g + 6, Xffi +*, a tr 8 .xJ tr e*. .ffis+,+*, *ffi*,& H tr. B E .
20、 xt E . + i6, Y b tE. fr E. tr #. ilt, FI 4. E H * . + ffi f . ffi ffi .E Ak ffi .W*# . a. lfr ffi . rK E b,Et,rs,H . H ffi . * rr ffi . rK H . f; I t . H ffi )r.S . + /r. tn . E tE er,ft,fr.ut . q a tr,wre#. r E* . 1&a & . H 5l . r|J fi . 7I E frJ . ffi E . q r, .+ ffi .# ffi .lf-ffi . ffi + . ffi
21、*. R,b4,rr.ffi . E ffi . E ffi . ffi * E . Hffi f, . il F E . *,) #. E# #. H f,+ . 4 E . + - n . F EE + . + + ffi .EUwwwwwwwwwwwwwwwwwwCt/1 22n-2dfr,5ffi,ffi, EffiffiS.,ffi.ffi:E.P.i$6.x,0ffi,ffi,#.#8.ftf ffiffi &,8m,#ffi9F#4E.4,ffiffi.,8ffi,#lm#ffi,dcffJ.-sffi.ff&,-Er-.&.#ff.ft.#ffirE,H#tm,&.,fffil
22、.frf,g.sg4.s,mffi*fifts,15.,8ffi ?ffi IK,lHffi *Xrl*i&,ffiffi, ft fl,ry . f,E*fi u,+ffiffifi.EhrffiHlvwwwwwwwwwwwwwwwwwwcJ/T 221-2005fiI fi i= zk tL IEJ- rE ttr & ffi , i*1 fiTfitriE A+ILryNgI !EI;T1.r #E+DNE*E T ffifitr UA +H ffLWJA A.H! UI E .+ tr EiE H T is zjc 4I E I- fl fit fi Hfe it yZ + W H t
23、lLW * E H! ifll E .1.2 Eyd ffLvr * aE ffi i5 iE + . +JLWr H,Bfr+r # A # bn. E E lr zK f &ffi A +tLli * M & Bt,H fi .1.3 FIEWW,+ fr Affi tr JA H ffi , W&tr84.88 H! H iHiE Ft, frW tK tljt Bt H ffi if E T zj Fdffi -h # T f trffi.trHffiF:HEEE,TI#ffiffiHf*fi/.tEiEffiHEtEE,HBBlfi.fr.4frp6rrfffi &ffiLfiiiH
24、a+JLVJ * B. HH ffLWJ iE trI tI 14 & i+ fI tr 7K + A ULW tr *Bt E tr, xf E JZ fr fi!.W&.fl1H e t E. E E,E X.1. 4 ttt*1.4. 1 Hfrffi:100 mL.1.4.2 Effidfl1.4.3 HfH1.4.4 q*,p 1.4.5 x+,ffiEt 0.001 g.1.5 *ffiNl EH ilLWJA E fi! # ff fi DrtllF & X7.4?+ tr* ffi.fE Jt zJ 6# E W.+ fi ffL *8, + r E H # ffi Htft
25、#,t+. X#B!ffiffi&tr,Rrlffifift. tnffifiE ,tfr.MWWEfi. 4c4ffiU(fH+ *#Ff IElFEffifi 24 h.1.6 frw1. 6. 1 ffi BiEEt *, ffiHt#ffi&X+LffiWlt to s H!ffiffi 1. 6. 2 WqBH + Fp ffJ W,fr ffiffi#.trYd ffi -L#, f* H f zl rl# Ht +, W H& /Wffi fi 1 03 t - 1 0 5 cHT 2 h, B H ffi +/*+$ fr W * yt o. s h tr ftt, EF)LW
26、, Hall.EEh *, 1. 6. 3 WH+ trH!#ffi ffiW,frffiffil.4rfrF f csso+ 50)cytffi | h,XH,ilH ffi tr ru ffiEp+Ezoo cfr.Ettfrfr ,ilAT,ffi*S,+*ptrffi6.h *, .1.7 itfrli w,+ d ilt wJ a a_ . ffiwE, lil %*.fi , &rt ( 1 ) if H,:ffixtoo% .( 1),tF,mz-tEH.H,Hffi inH Ttr ffi ffi W ffi,B.ffrH.E Sfit H ( e) ;* - tEEW.t#
27、ffi lnh ffi tr # F, ffJ ffi.a ffJ wH 4 i t f, ( e ) ;zz, -tEE Kfr ffiW ffi,E Ht &tr, Si fi ( g) .ttH-#X#mBJdff,fi trW&1.8 ,ffi#E5EffiE?lfr.6 t*&B,xf 10 f 6EWEiTUE# FA+tAmWAEnllEFI*&8tr+Hxf tdIEfH#t0.2%-t.7% wwwwwwwwwwwwwwwwwwct/r 221-20051.9 EHEFIE1. e. 1 H+IEEMmy tLH+trffrEt1#6Jt+ 0.001 g.1 . 9. 2
28、8.4 *F +, ffi 1 h fi Tfl,ffi ffi ,FJ ffiffi ft +ffi H, Ef IE-J EI JE g TE K fr ffi ffi 2 ffi,flFfrfr, Ark+fi0flUE EllE2.1 ffiE#fi tFil,tr-T H 6EB iNtI Efr fi tr UE tr H! 62K4.+ - E E H T li tK ,tW t fE & fr N fe i5 iE f zJ + Hn UtI E .2.2 E-y.W fr A ffJ E ft,# Fn tk4f6 4tr 6 B! # Em + + zl ird t,ff
29、f , ffi E 1 0 3 c - 1 0 5 CH ffi FI H AE E,mrtHtEE uH 1i+rf hfitft,*tba.2.3 TflE2.3.1 H#tsm.:1oo mL2.3.2 Hffi2.3.3 ftT,tsEt 02.3.4 Tffi*S.2.4 *ffiflEzjcx*H!ffiffiDfft*,t+.rf H6FEffirY Z+ 1,2.5 f.#2.5.1 ffiE2.5.2 XfTHfi,trIHI*eie,h *,tr H!i5JB*lR,H.EtBfi.ith m,2.6 i,+Hltffi+ Ht.( 2 )frF,*-friW,trJAHf
30、fim,-E-fi.tr*liffifizz, -IEEA#EmffitEtitH#R*.,frEzjffi,fi tr-&.2.7 ,ffisEruEffitrllfr. 7 + * & E xf 10 + 6 E W E It JIE H ffi H! A zj # U E, * & e A +H xf &n E ffi X.h o. 4 % -1.7% 3 fiIfiiirE ,EfifiErE*EHiflllE Er,*s. I fiE+n W *ntr-r H E E rE U E tr r( 4i E f. E ft, fi!, + ?E A & E flA W H ( MLSS)
31、 .4.8E ffi Ti6,i( &B T EA Wtr ffi W E E! UlI E 3.2 EylE A & E Jr, htE tzs frt E A Eft flU +n +frR iE A e fi ffi * A ffJ s4 fr. 0. 45 pm ffi ffi il ffi tr ffi ffi ,t+zm- (mz -mr)SiH(e);tH(s) wwwwwwwwwwwwwwwwwwcJ/T 221-2005frW,Wt6+rJ B!,H.6Gt 3.3 ItE3.3. I &mm.3.3.2 H+4.3.3.3 fifiHffiffi+3.3.4 x+,ffit
32、t o. oo1 g.3.3.5 Mffi.3.3. 6 ffiH,7L4e o. 45 pm, H.6 603.4 *Hmm 4lEISflffiEIEE+ffiffimUE MLSS H!H#&$JW&Xd*.+fiffI+-ffi,+fri)EHF ffi kl.ft#+ x#H!#ffitrtrFrltnwEilJ, U ErE&frW ffi.fitr &,FE lE F!hqt+&,MtE#& 43.5 frw3. s. 1 ,Hfiffosc#To.shEry.&,HT+f#sLffifuffi.EffiHilffi*$Ftffiffi3.5.2io mL #tEzlciS*ww
33、=ffi,E,&/ffiffih *r+13.6fr?7lzlll1v-+rH#*3.7 EHEFIE#Ht&ss4BEEFtSffi Exft, i&ftlHA,ElmfHrtryi# ffi3.8 ffi*EilEffiEffi E, d4E.J, 4rg ,tjfrffi ,f+fl %il. a f *&B,xf 11 +7FtrWHlE0.4%-2.1% & ittEWE H! ill E rf , q&E Fr +H xtffi E lffi#tJ4 ffifiitiE pH trHtNE E&,*4.1 fiE4. 1. 1 #t*fll,ET HH+ft1*W8ffifrY5/
34、ZH pH E4. 1. 2 +i-Ei6H Tfi rt?zK&L4rfrfr ffi Hei5 JE tr ft! pH E Ht UlI E.4. 1.3 +ri&iHffiH ffi Ht , H . iE H . ffi 6 WJ ffi ,F+y,fr1. tr H fi & & H a_ H E 4 6 + di W E ; E p H( 1 ff +A Ffi iH #)WE#, EI & mE UtI E ; pH 10 W P +- ffi*, EryfH ft ffi E H +ftJ ff) l*m# &H H +X, 4&.ffi 5H ffi Ht pH tr*E
35、iE ffi FttE*WW&xf fl+$it afr &.tr .3)A&FffiTf A6EIN Mffi 71ffi ffi fi Tfrfi E,E 8.,ffi AMffi +,ffirfiE ,F.E-*tfr-,HAtEEt 2,. ffiBtEEWE+lihli(mL).ffifi.*ftvKrl,WrcL)N&wwwwwwwwwwwwwwwwwwcJ/T 221-2005XFfibMA,Ifr,Ut.+,Jffi,F_1+,JE1,fr,#.+,JfiEE.#.TfiHE&TE,$I&E&fry.,nIxHEKE6DEf 14e.fr,t|ffi,#W W * lH h H
36、W nlq .ffi tr xf H fe H0 ts n fn pH ffiH FJ aE A E H ffi 15,fX #$ 60 +l H # E -5 H e H0 ffi H - #, + & A( Utt #ffi 5&EfX#$ Hffii;ntE#FHi&lHH# #.8*t c Z fi ffi tr, + A =Fkffi * ffi nlil p H H, * E _ F lt ffiiLflJ +,&t& t fl E Ffi til, X ff tr,1, rfr LEIJ iu EpH H.4.2 HrepH E H flU E H, ru, ffi H.dr *
37、 fr 1+ . u& H H dft h ffi H, dft , ffi ffi ff * H+h.h * rL ts tE rfl fi H ?U &Zsc*(+T,#i&+Nlkr t pH +i,tsi#e*.ir 5e. 16 mv,ffifta,fI*$tH*r,:t pH ffii*&*zr ffitr#FEX*t iqA?FH#E H fi -F.l-Lffi zK E i& tr JZ H ffi , ffi.% ffi-fr ft,* r0 u * 7fi +W tt 5i F, it B i& tr + ffi tr, W E rtrEf Ei pH .4.3 fit#
38、J4. 3. I +nE#i+EtrHtsCfirJilE4. 3. 1 . 1 E h +n +, *ffi Z;+ ElitEf+ffi fiW&.ftAffi ffi # pH br.tLttt ffiEt,E E Wj,nEE fl EH .4. 3. 1. 2 FtfttjtmtE#&.tfiffiffiq&ffi/(Df+ATrE*, ffiH+I$*p, BEBzJ ! 2 ps/cm B!,#fgzJ,H pH D) 6.7-8.3 2.tElttr.4.3. r. s inlE pH F-f ,&#ffigm,&,+,|tfflffi,|4=ffitrI6E,HFcffrl=
39、ffi pH fmlE#i&.4.3. 1.4 g&WffiffiB! pH EruH*ill*,nt,g4U# 1mff5H pH HtEItuHtffiEH&tr,fx*$.t t pH faE*fiffim,ftJ4,3.2 ffiEEtrH!#F4. 3. 2. l tnlE#i&4&#Lffiffi&lE*Hffi + M n Fs6 4. 3. 2. 2 E Effi,R+ T ffi & H #.- Wu &E t + E E z + E trr tr, fr.vLa E ia . E d J E fl*N,AEEW&ffi-H 4.3.2.3 AH& cy(ffifr#trr,
40、-H-HffklilrlE#&6rt i+EFJ tr* , i*#4roK&Hffi FE.4fiNWryJffipH(25C ) 1 ooo mL zlF&ffaHla.lBIEE(25C)E+tnlEmEwaffi(25crEfi)3. 5576. 4gKHC, Hn ()6trffiw.-affi5.tto11. 41 gKHzG HsOzs+:ryffiaffi4. 00810. l2eKHCsH.OaWW.-Afr+W&.A=ffi6. 8653. 388gKH, PO. o *3. 533gNaz HPO, (b)ffiw.-affi+&.a=ffi8.4131. lTgeKHz
41、POro +4. 3o2gNrz HpOnt2.4541.SgCa(OH)z )ti)wffiH.b Arooc-l3oc,HT2h ffi ffi #WrY#I+4 6trt- #4Lffi.?K a frt) *4w.= 4tr, &ffi ifr & ( 54 r s) t +,ffi , H +mtr 6EJiliil 60c .wwwwwwwwwwwwwwwwwwT(rc)ABCDE04. 0036. 9848. 5349.46453. 9996.9518. 5009. 395103. 9986. 9238.4729. 332l53.9996. 9008. 4489.276204.0
42、026.8818.429,q2 a4. 0086. 865o4139.180303.5524 0156. 8538. 4009. 139353. 5494.0246.8448. 3899.102383. 5484. 0306. 8408. 3849.081403.5474. 0356. 8388. 3809. 068453.5474.0476. 8348. 3739. 038503. 5494. 0606. 833B. 3679.011553. 5544.0756. 8348. 985603. 5604.0916. 8368. 962703. 5804.1266. 8458.921803. 6
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