1、GJ+ fp Ee + fn tr lfitErEig /t1!lfn;EcJ /T 322-2010ft# cJlT 3028. 1-3028.2-1994zlclLIE,H Effi fr.fr.#Ozone generator for water and waste water treatment2010-0 uq fr.fr2010-06-01 *tE+4pR,.ttfrtr ff.Bfisffi,?eiqff fr. frwwwwwwwwwwwwwwwwww.GtrIT 422-4.0mffie E i(ffi:#ffiffi*) .5,ffi,#dftffi$tfiif$ rq.i
2、r,.,i.rtr.,cniiri,!:!.i.iiir-ir.i.,iriii,-,i.m. 6ffi,*ecF,#, f,1, Hfi,H #&ffi#ffi&ffiffi# -.-,NrElwwwwwwwwwwwwwwwwwwct/T 322-2010+HUE+tnlEExf ct / T 3028. 1-1s e4( E H E4 * ) fE cl / T 3028. z-tse 4F fi, E 4 +$ R H W H . FE.HffiBiifitlA.bfr+lWif ,5 cI/T 3028. 1-1es4 fir cI/T 3028.2-tse4 tE tL+ENLlnT
3、 ,cl/T 3028.1-1ee4 ffi Cl/T 3028.2-7es+ ffir6 EP;jB fi r tis fnE-fl , 6, EEI T ft,+tn ffi fi # H! *ff ;-+Ffif PFoil#-ffitrt#;-WEi 4 & E*ffi HWfr * itttJtE*.i&)-E. &*I,FU ;-ffi E? T lF+.rfrfr Effi f inr g*, frLT F ffi Ht4* ;-flhr t.F,+*.X1afr6,-rin-rx+x*#ffi;-F&T EH *tr . PE . E ffi BIUII Efi if HtrE
4、 B! fi 6 ; Efi WHWEB nr T H tlWW.* ;ptIft A.B,igff rFff* c.+ffi ffi H! pfJ * A t *r ffi E ptl *, FfJ * B. pfj * c, ffi f+H ffiJ * + An IE Hfr ft ffi ffi 9 ift # fr zK fl F zj P ffi fr IE+L&*E * E n .*F,stEfr.frE H + n H.S E St* :11 &. FR ff ff A al .#br.W lnEH +U H # t+ q( Hfl + 5 r ER, + El r iL 4
5、W ffi 6 +E fi, + !t 4 -E * . H .S frE fi D,H I ffiffi.*ffi fr,+,1 . E f Et llt H W Fl 7K* T& A . tr fi ffi fi E H A- pE a A . iE e # t ffi 4xFt&fi. FRa A . Wffi =8 r6ffi fl+&a. pBa E .+an IE t4EH , T6Eg . + ry.,ts . r tsB . il., fl+ . rK # . rn & . ft # Bg . # A . ffi H & . E fi r .XJ-+,tt.Mr%#+ en
6、IE rEft * FrtE W ffi tr.ffi# Ffr H n -cl/T 3028. 1-1ee4;-cl/T 3028.2-tes4wwwwwwwwwwwwwwwwwwcJ/T 322-2010/(rtIE,tE EfiAfrEErffiE# Ft rEilF_T zF 4 4 ffi e H E e +F W rl Xfr *flffi , # fA ffi ffi F+ . 4 I . fi e - * . fit & *I ntJ An fi . &*.iaffifnE#.+tn ffi iE H + +.ffi 6 HzJ . F &zrk . tr zR 4 E ffi
7、 B! E H E & +$ .ft r H lL . #. eW H & A ffi I rlt iH6+H+EHffiEfiE+.#dI*tr.ffift 2 flfr,ff9tE*+ffr lbt*. 4 6 ffi Sl iH H! fr d ) *, b ir ffi 4 6 i6 H T + rt IE, f,* ffi , ff Er & E + ffi IE B fi Ur iI H! 6 h ffi X.E 6 r,l & H l*4 I + B! Eff ffi + rLE 6 E E ffi Hg 5 I H I tr, H &ffi ffi+i6 H T +ti g c
8、B 150 ffifitlEr#GB/T 1e1 *ffiiaKzr&rffiGB 3oes-1ee6 effr,4.ffi.t&nlEcB 4208 ,ffr,wF+&IP 419;GB/T 6682-2008 r|tfi *WEHzl*I,fiFilfi&.*GB ?szr. r-2005 ,fftEfr# *e&ffi?ffii,q6 6 t #h,4*fi&ffiffir4frfie8w&GB/T 13306 ffifficB 13384 t/rHrffi#iEHeft+GB 14050 Rfr*fr,fr14fr&EefiE*cB/r 1s438 ,6HA5 4HBtUE HfiJh
9、E*cB 1s517 EXH,frift6t+&*LfE3 ,rE+il8v.ffi.48ffiL=TrtI ti* fi EX . ffi . ffi ffi iEiE H T+,r IE .3. 1 fi+EEy.3. 1.1,IEFE+HtrH dielectric barrier discharge&.lt H t+E ffi E! H tE fn fi H A E, ffifril * r+ Ht ffi H EP e ffi 5.8fi fr,f,* 3.1.2Eg&+7E ozone generation unitF4Efi Ft#+ff +, H /t E,f+5&+r ffi
10、 Hf H&fl ffi E A FJ 4.fi .3. r.3Eg&tE ozone generation chamberh F-frB, * fr, HFEE +mH ffi,W #H 3. r.4E&tE* ozone generator1wwwwwwwwwwwwwwwwwwcJ/T 322-20103. 1.5H6,*fr, ozone systeme fi E 4 f . f;, UF # E . * f,4 tr & # E . E l000 Hz).eAftftm ,hhtufrH54e I+*p r*, ilt zJ I$*p fE a r ks/h).4.2 flfr&4.2
11、.1 HF.fr+.#ffiEEfiPE&ffiAt 1 H!fl,t.4.1.14. 1.24. 1.34. 1.4ature and pressureoE I EfiETEEffiEEgFIflI*HF,E*.#*4s-nffi,ffirJr4e/h5 10 15 20 25 30 40 50 70 85 100F4e/l200 300 400 500 700 800 I 000t4ke/1,1.5 2.0 2.5 3.0 4.0 5.0 6.0 7.0 8.0 10 t215 20 25 30 40 50 60 70 80 100,wwwwwwwwwwwwwwwwwwcJ/T 322-2
12、0104. 2. 2 E F . iTffi D ffi,ftfr H fAffi Am P F, +ilrH nH& fr S *flffi + tE 6EE .s #+E&ffi#+5. I H+E5. 1. 1 HFX.+ #&EHE4A,FfrHffi .r+*p*E.frfi|*85It+4.fi 5. 1. 2 flHfr+.#f8 lfrffi tr EDH*l+frlrrl&HH.4fr,W.&E*E* s. I . 3 R + E )r * Bt 4 fi E 4 ED & E, 6 * 4 * ffirfi ttil,lrn r . fiS &, * #L+ E )r #
13、* &W ir.iEffrlflffiYt+.5. r. 4 HHfr*.8fr+rrfvfi MAtlLffiffiffi,xIT+nffirH&#E/ffit*+&Wfrtfr.tbF.,MH.WH.6fiLt f & tr Hi s %, tbH-NH 6 zJ T 1 /3, ZF IlJ & +lH, H&*iF + g 5. l. 5 Efl E4+F&AA4.fnEiqEffi E . E7: . ffi E+&U,fXt, fi$U Efi tft,ffi E. &EX*6ry 5 Aft U ft, fi ffi H 6! re A, ffi fr.fr,E X t B! E
14、 En E ( E E fi, fr. +.afr.ffi 4 fr 5 ffi ) s. r. 6 FfiEe*&44UE&EA)eB! E lr .,fXtS ,*flHH.4btffiEE9rfltr .5. 1.7 4H&4*fFffi ft,iftaHtiqil.Dffia GB 1ss17 E!*IE.5. 1.8 ,t.tr48flfr.+.#ilHffiffiF+W.rfrffiA GB 4208 #JFI,E-,6DftT IP44.5. 1. e t.tr4Ffl E+#H&,a) ,6HffiE6HT as C ,fExf&ET.Ht 8s%;b) I$*FzJffzJc
15、mH;FtT 35 c.6.2 trftffi6. 2. 1 f,FE+.#xf6*f;,ilF*n# 2 tz fr55ffiffiffiffiff+#F,Eh/vrPH,8ffi,/CF.a,w#,+ry./%=5,)-0.2(-ss2745, PSA/VPSA ftfi(1 m3lh)-0.7e027 m3/h0.20.259e.66.2.2 rfi4g6,X.4*Fftffimfi/ffiH6ft+ o. 1 rlm H!ffffi,#E.wwwwwwwwwwwwwwwwwwcJ/T 322-20106.3 Afl?k6. 3. 1 H&r+*p Efi E4 *$ B! I+*zJ
16、*,H rl W.WB (fX+$ * ) ru E E fi * E, & Et E q(+ *) tF, + & - E F4EFEHF.WE / G/n)EfiEffi/(kwh/ke)a5,m1fii +. z i&E)18flft.TH(& 4.2 EE)100e(fii 4.2frft)15011E 1, t4FflEt+.#ffJffiED$Elfi(cosd)6&zjrT o. gzE 2, zJr4Efl Ee*F ffi ffi E&#ArFJi6 g EFfft wwwwwwwwwwwwwwwwwwcJ/T 322-20107.2 EfiFIflJE7.2.1 fi*,E
17、 rf WJ E E H E 4 # B! E fi M H X E fi ,f-15 ffi E, Tf H E fi * E ffi tr 5 F fi L f;, ffi E (T E II # )&rq*fl, EptEHPE&tr.7.2.2 i+HrtEfiPEEfr(1)itH.D:C.Q ( 1)fr+,D-FHP Et e/h t44fi84,* EEEHFEEH&Hfi kelh #zr ;c-R g W H, s / m *, re / L, #An IE X H tr IE tt # f B! rF E * H ;a-Hfi4l,ffiE ,m3 /h7.2.3 Eg.
18、ftf tElilrtE+ o. z c uJ 6 . iltl + B! ft, f ffi Efi & ffi Eii Et # 4 trfr fr.H. 8)r B rti+ H-, rS Bi tr E )tt # H! ffi t 8 .ffi EirE* E HF.E4.g tr ffi 89, fi 6 ft,i+ffi AM&H h fr 5. ffi E fi 4L ft ffi E . f, l+ B E *,e.*wnFf!* n.7.3 EH#fl|lEiE H F fl H ffi,Lvw X. Hfl E e # H 9 rr. H E E #E 69 fiA, 6
19、 ffi AUF fill 6 fl +,fU tEJ & ffi 7.3. 1 f i*E rf U E E fl E E f H! E H P E X, EE H H E E N fr+J dJ rJJ 4, iT H- W. /l + 5 E fi P E B! tT EPTEHHffi.7.3.2 i+H*EEft&fr(2)itH.P:Y .( z )fr+,P-Efltsffi,kw. h/ks;w-ArJfi4,kw;D-Efif Et kelh.7.3.3 flllEE*7.3.3. I EHFE&, 7.2 ffi*AEellE7 . 3. 3. 2 E ir tl 44 H
20、 & CIt * (ffi * ) A 4t 4 fr + * Ur 4*., &EI X. ffi *A fr?fr,E #rH AA +fJ W:R,NWffiEtr.MjAx 0.5 W.7.3.3.3 gFHE&#HtFfiPEffiErf ,4H H,6E#( H,Et)UE Fh.+.#&-erf l tr iHffiB!Apl H 6EE, rtr EEEtsrf H rf E fr+J W,trhd 4rh$tr 7.3.3.4 ;,C. +4EfiEe*#D IFJ rfw Ath+B*.7.4 ffiEfrA+EtrfiffiBEatrE H E4 #$ HE ffi Ee
21、 rH &f & fl D re A 6. 1. 1 4* Hfik+.#D&iqii 6! ffiftA *e.trft ffi EHiIN,Ttr,6.EHWtre 7. 1&ilU,EHFEI& 7.2 &U|I,HHHffi& 7.3 f&il.7.5 Er&flllHfifreg.Erfitiru&rea GB 150 F!fl,E(wwwwwwwwwwwwwwwwwwcJ/T 322-20107.6 f;,ffittHFEt+.8ffi,8D&A GB 1s0 B!*LE.7.7 HEttHF,E*.+*E;fr 4 htr,Aift,lffiffiftrJB&trEffiEflr
22、frT,2 hFtE.)-flE 5 n(rf l4+4A6 ) E H W H fl H ffi Utl E E + & Jt 5 & 4 ffifr+r EW t+ qE, ffi 1+# R EP tJ N.Ar E 7.8 EEitrFi& GB/T 1s438 WE. EffiHEfr nffi 1.0 * ffiE.1.0 m Htr&UlIEHIEffiE.7.9 iEffTTBEerE. HFfr*. *$ tr flxfiw.rlt E (,fX+F E ), f/ft.T &EE&flWtr+t&H-ffrfr*L.2 BIEL.2.1 EIIEfi(O,)E-H#xtw&
23、ffi4t,6,HBfiWH) &ffiDilftffi&ffiHEv&A.1 )4.2 )a.2.2 ttW1FfrL.2.2.1ffi+|,ffitr,$ffi.frREffia.2.2.2EtE 1ta.2.2. a ffiftffiW.250 effi,&,ffi,I+ffi.EE t l-.EM+A.2.2.4 HffiUTffiffa) f,t#E#)ffiarilJIil a e rf66#trfuArtttryrffi fi fUA 20 e H,ll,* (ZnCl,) ffi100 mL friL+ Wf i+WW,#ffi,H4+ffiWl4100 mL. &tr,ffi
24、W&ffiF51 L,+fiA2 e A,4L* (zncrz). +ffi zrilJE&)E4I gmqffift-Rtr=+ E b) EffiffiMilJrfu 5 e 4HE# + ril /- 1+fr7K, Xffi,#affi)tt. ffi ffi fi W BJ L t L #,W W,IK+, ffi #, + m&ffiE. BHr.iHY&,Sffi.L.2.2.5 ffiftffim$(Na,S,o. . 5H,o)iHEfiW Ee f;, ffi Ffl Wtr rf ffi #ffi ft ffi ffi fr ( Na, S, O, ) ffi E V&
25、W tr t o. 1 mol/L ; W E fi ft, UH F H #trFJ,ffi#ffift6ilmfr (Naz$o, )ffiEy&*Ht o. s mot/La) mffiJ 0. I mol/L Amftffimfi(NazSzOs)ffi8& EB 100 mL Wtrt 1 mol/L EE Na,S,O3 FtF&T soo mLffi#Wl$*nBtgtzlcf ;b) mftl 0. 3 mol/L ffiftffimfr(NazS,Or)ffi8& EB 300 mL WH.h 1 mol/L Et Na,S,O, Fffi&T 7oo .L ffi#ffiI
26、$*fttfr,tkf 8EH&rut,fl , 5M+Lffi (KI) zJcF& E-fit/. kWHm ( I, ) .fr ( Na, S, o, ) ffi E&rf ffi H&trfrffi E (Q0%,03 .5H,o)Ff#HiE(!t I moVL)(Naz Sz Or . 5H,O),HT#ff WI+*p HtgtwwwwwwwwwwwwwwwwwwcJ/T 322-2010A.2. 2.6 !#&fi(KzCrzOz)#fi(0. 016 67 mot/L)ffi.Httffi*+tffiffiWgS.105 c-110 cfiT 2 h,*#&Tffi*F+A
27、*p 30 min DJt HgEffSffifr(ffi*.fr)4. e04 c,EWf 1 000 mL6gffitrffi ffiifiil1ffi.R*A.2.2.7 flftffiff(Kro3)EfFa.2.2.8 Z*(CH3COOH)A.2.2.9 fr7kfrrflfrreA cB/T 6682-2008 =*tLfflfl,E,E+6H+ o. b0 mS/m.A.2.3 ifiBTP.iEE E*A.2.3.1 Jiffi7+,ffiHt o. 1A.2. 3.2 EfffiIEffia.2.3.3 ffiEB 50A.2.3.4 Wffitfr.&E)r*.ffiif
28、lUErtffi&#fr.+o.z cA.2.s.5 ta.2.3.64.2.3.7a.2.3. 8a.2.3.9L.2.4&H,E.NUfiHa)WfiBTft,fi,016 67 mol/L0 mL E#)tr6milJffift:. (A.3 )*F,B-ffift6mffiN-EfiFffitr16E% -6htailffifrffiEy&iHffiE;v, -WHE.W&.fr tpnB# y& B! +fl , mL.b) fr 250 mL ffiMffi+ in so mL W,tK,#*ffi#f , iu o. o7i g ffi&# (Kro, ) fE 1. 5 e w
29、4t6,fr(KI) ,f*E?lfi so mL fr,tf tEAtr nlA to mL L&. xf f4fr89ffi,&HmfftI*HBlDhtffimffiffif &ffiE5,t,JL+iHtr frE 1. 0 mL EIS#milJ,44zJ,L.ffiEaffieEUiF iH*.,*#& 30 s T4Etffi,ffi t6ffi mffi ffiE& B!*H&fr (A. 4tlH- o: w - - v x274.00/6 000 -*FB-0ilftffi mffi Bi E &WH, mot/ L ;W-&ffi#fl BOEEI, g;v-6iltdh
30、ffi ffi ffift e 6! iH ffiE, mL.0.016 67 mol/L;le.E.B!H.6ilft:d/(Ev&89Wtr&fre. 3)itH yx 0.035 67wwwwwwwwwwwwwwwwwwcJ/T 322-2010& t t &r E tE + ffi HilJ H E ( ffi E 6F&H W & . & e tr tr + fE &4t# tr + ) E A T Dil ft ffi m fr ffi EW.W E E1t 0. 1 mol/L r.f # # B! H E, * ffi Fi ifij H E & # mft! Fi dffi
31、ftmffi fr ffi E v& Ht * E ff ? rfl # ( fi ffi ft 6h m fiwE911h 0. 3 mor/L r,f ,fiillHEEjfgilE 3 ffiafr) a.z.s it&Etr&r*A.2. s. r &fia) iIfl#iE*mtTirr+.b) *frwA. 1 E&EH5,+UfiH&n6.i-&FE&*;2-EE;3_E)1;5a_aFE;5-s5lfE;6-&frffiErl.E A. 1 Eg&ei*u5,EE*trflUrt#Ec) &,Hffi+$hftffiA+stft,IFnnA +o mL 20%trJ KI Hy
32、&fE 360 mL 4zJ.d) fr 50 mL &ffiffiE+EA4trrEB!ffitffimffiffiEfe . fr*WIfr.AeAiE ffift,#HHf tr,fT, ffi E tr fiIA H!ffiE&AD ffi X&,ffi .a.2.5.2 *ffiA. 2.5. 2. 1 WHF+LE!Btrffi TUA H#5,ffi +,&Hff4ffi Ffl S&HH. ftr,ffiEfiHffitrHEtr5ilI E#ft,ffi EH, #r, Ep &H e*mEil+lf iE *+fl .2.s.2.2 D) 7 L/min BIEHlhlff
33、i5ffi+ffA 1 L-3 L 8fi5+ ,X#Wffi#-t,its*ffifrffiEif B!&ry.88 +Et * & rE 6! 5+trR . ffi # Bt + 6 fl E * T e fi * H . ffi E ve f fl fn ffi ft ffi m fr W H g trft, ffi # te.ffi E wwffi#-*rf , w i& H!,ffi trfi H A.2.5.2.3 W#frE RtrE+ffit,ffi+ffifinrf- s mL ffiffiHY&(1+5) U&H&F! pH EFfiftfr 2 UT ,+*A ,ffi
34、E 5 minA.2.5.3 iHE. 2. s. 3. 1 Bf #ft,fn + H! Wy& W &E- + 2 L frtJ ffiMffi. ffi fr.tKfr,lt$ffi ffi ,ffi 3 tr, *tr F UEtrfr 4.7K W WTffiM ffi+ E* &W y& Bt ilE +, & tr 4 BE d 4 &6ffi fr hD Lt+ .A. 2. 5. 3. 2 id *ffi E tr ffi .ft & m ffi ffi E v& Hi uJ rfr trtr, & H ffi ,ft ffi m fr ffi E a E v& A t &
35、it 6 .fi wMffi + frn 9A1 s mL EldlHfiJ, H &* fi 4,it ffi 6 zJ,L ffi E, -.ffi -ffi rUff fi, HE# e E ElllHft,_EH&i$iil,+ffifi 30 s 64trffi,.A. 2. 5. 3. 3 iE *ffi E fr+re.*&W., *I+H-4F.EJ&H H! ffi E r&+fl . its *ffi ,tr Bi ffi E e+fl ffi ffi Ev&6t*ffiwE a.2.6 Eg*Ei+HA.2.6.1 ffiEE, tbtr trBtJ,+ERefr (A.
36、 s)itH.10awwwwwwwwwwwwwwwwwwct/T 322-2010tl -rl x(P-f,+P.)r.Ty. (A.s)P*r, Ttt+,v*, -&i IE ffi H E.i # + T B! f;ffi l#ff, L ;v-*&E 6!f;,6+R, H &fr mEitill $, L ;P*-&ilEf;,E*Hc: y .( A.7 )Y NTPfrFC-Rfl HlEE*tr, e/ m (me/L) ;M-& KI EITEIEHEE,Mg, Hfr(A. 6)itHlS9J ;v*,-&ilE)tt# FI H!ft f +fl , L, H fr (A
37、. s ) itH+9J .2.6.4 &E*Ullftffitr#fr ftUUHH*WffiH#.+z%tilfr T A. I TEEET?KHTTflfE*H,Emtr/c*frE/kPaWE./1l#nEikPaffiH_/t#itE/kPaEtr/#fi8/kPaffitr/cffiiE/kPa10. 01.2372.61.46t5.21.7317.82.0420.42.4010.27.24t2.81.4815. 4t.7518. 02.0620.62.4s10.47.2613.01. 5015. 6t.7 718.22.0920.82.4610. 61.287s.21.5215.
38、8t.7918. 42. t227.02.4910. 81. 3013.41.5416 01.8218,62.1421.2o co11.01. 3113.61- 5676.21.8418. 82. t721.4D trCrt.21. 3313.81. 5816. 41.8619.02.2027.62.5811. 41- 3514. 01.6016.61.89t9.22.2227.82.6711.61. 36t4.27.6216.81.9119.42.2522.02.6411.81.3814.41.64t7.01.9419.62.28,t,2.6712.0l. 4014. 61.66t7.2I.
39、9619.82.3722.42.7112.21.4214. 81.6817.41.9920.02.3422- 6t2.4t.4415.01.7017.62.0120.2L. JI22.82.7711wwwwwwwwwwwwwwwwwwta. 1(&)mtr/C*fr8/kPamtr/C*itE/kPamE/C#itE/kPaffitr/t*ffiE/kPamtr/c*fr8/kPa23.02.8t25.43.2427 .83.7 330_ 24.2932.64.92o2,2.8425.63.2828.03.7830- 44.3432.84.9723.42.8825.83.3228.23.823
40、0. 64. 3933.05. 0323.62.9126.03. 3628.43.87s0. 84.4433.25. 0823.82.9526.23. 4028.63.9131.04.4933. 45. l424.02.9826.43.4428.83.9637.24.5433. 65.2024.23.0226.63. 4829. O4. 0031. 44. 59s3. 85.2624.43. 0526. 83.5229.24. 0531.64. 6534. 05.3224.63. 092?.03_ 5629.44. 1031.84.7034.25. 3824.83- 1327.23. 6l29
41、. 64.1532.04. ?534.45.4425. 03. l727.43. 6529.84.1932.24. 8134. 65. 5025.23.2027.63. 6930. 04.2432.44. 8634. 85. 56cJ/T 322-2010a.3 *rFe&,tA.3. I HEe fi xf 25 4 nm &K ffi XrF )bA #ffiWW. HHt+,ffi tr ffi I tt + ( 6 A E H B! A 5, 4 H,5 ) A,U p-t tr E H! ffi E tr t. * H! ry & &, A ffi ft. iE ff & t& ru
42、 r.J & )E & U # & U B! )E ffi t r., # ffi 5 iE tr ryeiurf atfeu+#&ull $!/6rq t,r / ro tE/6s ,fx# B!ffi&Lga%ffifrHffi-P.,rxftjei+H H EH*tr,it&tzFjFt:6 Hfr(A. 8)4fr(A. e)tfr !:.- (A.8)roc:-1.I.r/I) . (A.e)a L Io ifr+C-RfiH! WffiIIf-;-Rfl &rnlE*t#Txt 254 nm WKX rI JtW WW.Afi , a: 308 ;L-W.W.fuI6EFKE *;
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