1、 File .ta20182018071020180710YFB5686-003-1_2.D Tgt Mass (CHM):Injection Date : 10 Jul 18 8:28 am +0800 Seq. Line : 8Sample Name : YFB5686-003-1_2 Location : P1-A-07Acq. Operator : SYSTEM Inj : 1Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:LCMS03Data201820180710201807101-POS-3MIN.
2、MAnalysis Method : D:LCMS03Data201820180710201807101-POS-3MIN.MCatalog No : HY-100741 Batch#31404Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um A-RP-186Oven Temperature : 45Cmin0 0.5 1 1.5 2 2.5
3、mAU0250500DAD1 A, Sig=214,4 Ref=off1.5441.6181.802min0 0.5 1 1.5 2 2.5mAU050100DAD1 B, Sig=254,4 Ref=off1.5441.6181.8152.029min0 0.5 1 1.5 2 2.5mV0100ELS1 A, ELSD Signal1.696min0 0.5 1 1.5 2 2.5010000002000000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.6591.842min0 0.5 1 1.5 2 2.50100000200000300
4、000Ion 830.3, MSD1 830.3,Target Mass 829.3 +H Positive, EIC=830:8311.660Integration Results for DAD1 A, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.54 0.02 1.51 1.23 0.10 2331.62 0.03 1587.86 826.70 99.85 8291.80 0.02 0.88 0.09 0.06 282Integration Results for DAD1 B, Sig=254,
5、4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.54 0.02 0.36 0.32 0.11 2331.62 0.03 335.70 174.65 99.56 8291.82 0.02 0.46 0.39 0.14 2822.03 0.02 0.65 0.66 0.19 233Integration Results for ELS1 A, ELSD SignalRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.70 0.06 724.64 207.81 100.00 82
6、9MS Report from Instrument: LCMS-03LCMS-03 7/10/2018 9:16:57 AM SYSTEM Page 1 of 4Integration Results for MSD1 TIC, MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.66 0.08 10254762.00 2218330.00 98.66 8291.84 0.05 139642.55 51979.43 1.34 282MS Report from Instrument: LCMS-03LCMS-03 7/10/20
7、18 9:16:57 AM SYSTEM Page 2 of 4Ret. Time: 1.66 m/z100 200 300 400 500 600 700 800 9000250005000075000100000125000150000175000ES-API Positive833.2415.9830.2415.2829.2Ret. Time: 1.84m/z100 200 300 400 500 600 700 80005000100001500020000250003000035000ES-API Positive102.1830.2415.2141.1 338.3283.2105.1233.1282.2MS Report from Instrument: LCMS-03LCMS-03 7/10/2018 9:16:57 AM SYSTEM Page 3 of 4* End of Report *MS Report from Instrument: LCMS-03LCMS-03 7/10/2018 9:16:57 AM SYSTEM Page 4 of 4
