1、 File .0182018031520180315-2CPK2018-315-08205.D Tgt Mass (CHM):Injection Date : 15 Mar 18 9:56 pm +0800 Seq. Line : 86Sample Name : CPK2018-315-08205 Location : P2-C-01Acq. Operator : SYSTEM Inj : 1Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:LCMS03Data20182018031520180315-21-POS
2、-3MIN.MAnalysis Method : D:LCMS03Data20182018031520180315-21-POS-3MIN.MCatalog No : HY-12008 Batch#08205Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um A-RP-186Oven Temperature : 45Cmin0 0.5 1 1.
3、5 2 2.5mAU0500DAD1 A, Sig=214,4 Ref=off1.3721.4331.4471.632min0 0.5 1 1.5 2 2.5mAU0500DAD1 B, Sig=254,4 Ref=off1.3031.3421.3721.4531.632min0 0.5 1 1.5 2 2.5mV50100ELS1 A, ELSD Signal1.441min0 0.5 1 1.5 2 2.5010000002000000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.402min0 0.5 1 1.5 2 2.5010000Io
4、n 430.9, MSD1 430.9,Target Mass 429.9 +H Positive, EIC=430.6:431.6Integration Results for DAD1 A, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.37 0.02 1241.43 1152.72 99.59 3941.43 0.01 1.79 2.69 0.14 3941.45 0.02 2.45 1.74 0.20 3941.63 0.02 0.86 0.09 0.07 233Integration Resul
5、ts for DAD1 B, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.30 0.01 0.06 -0.01 0.00 2331.34 0.01 0.04 0.09 0.00 3941.37 0.02 1202.69 1119.04 99.93 3941.45 0.01 0.30 0.37 0.03 3941.63 0.01 0.45 0.02 0.04 233Integration Results for ELS1 A, ELSD SignalRetTim Width Area Height Are
6、a% MS(+)|-|-|-|-|-|-|MS Report from Instrument: LCMS-03LCMS-03 3/16/2018 10:37:20 AM SYSTEM Page 1 of 41.44 0.05 490.65 159.27 100.00 394Integration Results for MSD1 TIC, MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.40 0.06 9397589.00 2381118.25 100.00 394MS Report from Instrument: LCMS
7、-03LCMS-03 3/16/2018 10:37:20 AM SYSTEM Page 2 of 4Ret. Time: 1.40 m/z100 200 300 400 500 600 700 800 9000250005000075000100000125000150000175000200000225000ES-API Positive416.2395.2394.2MS Report from Instrument: LCMS-03LCMS-03 3/16/2018 10:37:20 AM SYSTEM Page 3 of 4* End of Report *MS Report from Instrument: LCMS-03LCMS-03 3/16/2018 10:37:20 AM SYSTEM Page 4 of 4
