1、 File .ata2017091920170919-2BIZ2017-919-WYQ15.D Tgt Mass (CHM):Injection Date : 19 Sep 17 6:14 pm +0800 Seq. Line : 49Sample Name : BIZ2017-919-WYQ15 Location : P2-D-07Acq. Operator : SYSTEM Inj : 1Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:LCMS03Data2017091920170919-21-POS-3MI
2、N.MAnalysis Method : D:LCMS03Data2017091920170919-21-POS-3MIN.MCatalog No : HY-14247A Batch#26349Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um A-RP-186Oven Temperature : 45Cmin0 0.5 1 1.5 2 2.5
3、mAU0250500DAD1 A, Sig=214,4 Ref=off1.1181.3951.6071.790min0 0.5 1 1.5 2 2.5mAU020DAD1 B, Sig=254,4 Ref=offmin0 0.5 1 1.5 2 2.5mV50ELS1 A, ELSD Signal1.178min0 0.5 1 1.5 2 2.50200000040000006000000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.141min0 0.5 1 1.5 2 2.5010002000Ion 223.1, MSD1 223.1,Tar
4、get Mass 223.1 Positive, EIC=222.8:223.8Integration Results for DAD1 A, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.12 0.02 1098.80 819.52 99.78 2241.39 0.01 0.88 1.47 0.08 2241.61 0.01 0.54 0.80 0.05 2241.79 0.01 0.98 -0.00 0.09 195Integration Results for DAD1 B, Sig=254,4 R
5、ef=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|Integration Results for MSD1 TIC, MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.14 0.06 28218756.00 6965844.50 100.00 224MS Report from Instrument: LCMS-03LCMS-03 9/20/2017 10:04:04 SYSTEM Page 1 of 3Ret. Time: 1.14 m/z100 200 300 400 500 600 700 800 90002000004000006000008000001E61.2E61.4E6ES-API Positive225.1224.1MS Report from Instrument: LCMS-03LCMS-03 9/20/2017 10:04:04 SYSTEM Page 2 of 3* End of Report *MS Report from Instrument: LCMS-03LCMS-03 9/20/2017 10:04:04 SYSTEM Page 3 of 3
