1、 File .1-1 2018-02-01 15-18-45CPK2018-131-09095.D Tgt Mass (CHM): Injection Date : 1 Feb 18 7:58 pm +0800 Seq. Line : 59Sample Name : CPK2018-131-09095 Location : P1-A-04Acq. Operator : HCL_771 Inj : 1Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:chem321DATA2018020120180201-1 2018
2、-02-01 15-18-451-POS-3MIN-1.MAnalysis Method : D:CHEM321DATA2018020120180201-1 2018-02-01 15-18-451-POS-3MIN-1.MCatalog No : HY-14445 Batch#09095 A-RP-189Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm
3、,3.5um A-RP-186Oven Temperature : 45Cmin0.5 1 1.5 2 2.5mAU0250500750DAD1 B, Sig=214,4 Ref=off 1.5201.5651.7541.9231.947min0.5 1 1.5 2 2.5mAU0200400600DAD1 C, Sig=254,4 Ref=off 1.5371.5651.7541.9081.947min0.5 1 1.5 2 2.5050000100000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.785min0.5 1 1.5 2 2.50
4、200004000060000Ion 342.3, MSD1 342.3,Target Mass 341.3 +H Positive, EIC=342:343 1.782Integration Results for DAD1 B, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.52 0.03 6.28 0.16 0.38 ND1.57 0.03 23.99 16.07 1.44 ND1.75 0.02 1626.73 1187.92 97.56 3421.92 0.03 3.67 3.26 0.22 N
5、D1.95 0.04 6.80 3.57 0.41 NDIntegration Results for DAD1 C, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.54 0.02 3.61 3.15 0.34 ND1.56 0.02 12.01 8.44 1.14 ND1.75 0.02 1030.31 754.32 98.06 3421.91 0.03 1.45 0.04 0.14 ND1.95 0.04 3.35 1.71 0.32 NDIntegration Results for MSD1 TI
6、C, MS FileRetTim Width Area Height Area% MS(+)MS Report from Instrument: LCMS-02LCMS-02 2/2/2018 15:08:50 XLH_854 Page 1 of 3|-|-|-|-|-|-|1.78 0.04 310165.25 134283.69 100.00 342MS Report from Instrument: LCMS-02LCMS-02 2/2/2018 15:08:50 XLH_854 Page 2 of 3Ret. Time: 1.78 m/z200 300 400 500 600 700 800 900025005000750010000125001500017500ES-API Positive344.0 365.0364.0342.0MS Report from Instrument: LCMS-02LCMS-02 2/2/2018 15:08:50 XLH_854 Page 3 of 3
