1、 File .20182018062220180622CPK2018-621-10560.D Tgt Mass (CHM):Injection Date : 22 Jun 18 9:49 am +0800 Seq. Line : 20Sample Name : CPK2018-621-10560 Location : P1-A-11Acq. Operator : SYSTEM Inj : 1Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:LCMS03Data201820180622201806221-POS-3M
2、IN.MAnalysis Method : D:LCMS03Data201820180622201806221-POS-3MIN.MCatalog No : HY-50948 Batch#105600Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um A-RP-186Oven Temperature : 45Cmin0 0.5 1 1.5 2
3、2.5mAU05001000DAD1 A, Sig=214,4 Ref=off1.2151.3621.4541.5291.792min0 0.5 1 1.5 2 2.5mV050100150ELS1 A, ELSD Signal1.433min0 0.5 1 1.5 2 2.505000001000000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.393min0 0.5 1 1.5 2 2.50200400Ion 432.9, MSD1 432.9,Target Mass 431.9 +H Positive, EIC=432.6:433.6In
4、tegration Results for DAD1 A, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.22 0.02 4.47 4.20 0.26 1301.36 0.02 1712.38 1597.03 99.05 3961.45 0.03 2.14 0.76 0.12 3961.53 0.02 8.01 8.11 0.46 2331.79 0.02 1.72 1.29 0.10 233Integration Results for ELS1 A, ELSD SignalRetTim Width A
5、rea Height Area% MS(+)|-|-|-|-|-|-|1.43 0.05 610.87 198.78 100.00 396Integration Results for MSD1 TIC, MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.39 0.06 4987924.50 1363733.25 100.00 396MS Report from Instrument: LCMS-03LCMS-03 6/22/2018 10:22:04 AM SYSTEM Page 1 of 3Ret. Time: 1.39 m/z100 200 300 400 500 600 700 800 900020000400006000080000100000ES-API Positive813.3342.1397.2396.2MS Report from Instrument: LCMS-03LCMS-03 6/22/2018 10:22:04 AM SYSTEM Page 2 of 3* End of Report *MS Report from Instrument: LCMS-03LCMS-03 6/22/2018 10:22:04 AM SYSTEM Page 3 of 3
