1、 File .Data2018010920180109BIZ2018-109-XT2.D Tgt Mass (CHM):Injection Date : 9 Jan 18 6:51 pm +0800 Seq. Line : 118Sample Name : BIZ2018-109-XT2 Location : P2-A-01Acq. Operator : SYSTEM Inj : 1Spec. Reported : MS Integration Inj Volume : 8 ulAcq. Method : D:LCMS03Data20180109201801091-POS-3MIN.MAnal
2、ysis Method : D:LCMS03Data20180109201801091-POS-3MIN.MCatalog No : HY-107145A Batch#28166Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um A-RP-186Oven Temperature : 45Cmin0 0.5 1 1.5 2 2.5mAU01000
3、2000DAD1 A, Sig=214,4 Ref=off1.3521.385 1.4331.4651.4821.8762.0332.209min0 0.5 1 1.5 2 2.5mAU0200400DAD1 B, Sig=254,4 Ref=off1.3981.4331.4821.5321.6071.6611.7561.8722.031min0 0.5 1 1.5 2 2.5mV2550ELS1 A, ELSD Signal1.502min0 0.5 1 1.5 2 2.510000002000000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701
4、.467min0 0.5 1 1.5 2 2.50100200Ion 729.2, MSD1 729.2,Target Mass 728.2 +H Positive, EIC=728.9:729.9Integration Results for DAD1 A, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.35 0.03 3.03 1.60 0.33 1571.38 0.02 1.96 0.05 0.21 1571.43 0.02 887.66 723.09 95.53 1571.46 0.01 23.7
5、8 35.85 2.56 1571.48 0.01 11.13 13.79 1.20 1571.88 0.01 0.41 0.48 0.04 1572.03 0.02 0.75 0.62 0.08 1572.21 0.02 0.48 0.07 0.05 105Integration Results for DAD1 B, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.40 0.02 1.18 1.30 0.17 1571.43 0.02 671.52 538.95 98.75 1571.48 0.01 3
6、.46 5.02 0.51 1571.53 0.02 0.17 0.12 0.03 1571.61 0.02 0.69 0.61 0.10 1571.66 0.01 0.13 0.14 0.02 157MS Report from Instrument: LCMS-03LCMS-03 1/10/2018 9:21:19 AM SYSTEM Page 1 of 41.76 0.02 0.47 0.19 0.07 1571.87 0.02 0.40 0.30 0.06 1572.03 0.02 2.01 1.87 0.30 157Integration Results for MSD1 TIC,
7、MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.47 0.06 2802785.00 798381.06 100.00 157MS Report from Instrument: LCMS-03LCMS-03 1/10/2018 9:21:19 AM SYSTEM Page 2 of 4Ret. Time: 1.47 m/z100 200 300 400 500 600 700 800 9000100000200000300000400000500000600000700000ES-API Positive158.1558.2557.3157.1MS Report from Instrument: LCMS-03LCMS-03 1/10/2018 9:21:19 AM SYSTEM Page 3 of 4* End of Report *MS Report from Instrument: LCMS-03LCMS-03 1/10/2018 9:21:19 AM SYSTEM Page 4 of 4
