1、 File .130-5 2018-01-30 16-03-28BIZ2018-130-XT3.D Tgt Mass (CHM): Injection Date : 30 Jan 18 4:19 pm +0800 Seq. Line : 4Sample Name : BIZ2018-130-XT3 Location : P1-B-07Acq. Operator : XLH_854 Inj : 1Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:chem321DATA20180130-5 2018-01-30 16-
2、03-281-POS-3MIN-1.MAnalysis Method : D:CHEM321DATA20180130-5 2018-01-30 16-03-281-POS-3MIN-1.MCatalog No : HY-115038 Batch#28493Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um A-RP-186Oven Temper
3、ature : 45Cmin0.5 1 1.5 2 2.5mAU02505007501000DAD1 B, Sig=214,4 Ref=off 1.6681.767min0.5 1 1.5 2 2.5mAU0100200DAD1 C, Sig=254,4 Ref=off 1.6521.767min0.5 1 1.5 2 2.50250005000075000100000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.792min0.5 1 1.5 2 2.5010000200003000040000Ion 252, MSD1 252,Target
4、Mass 251 +H Positive, EIC=251.7:252.7 1.793Integration Results for DAD1 B, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.67 0.03 4.09 2.55 0.23 ND1.77 0.02 1739.54 1263.05 99.77 252Integration Results for DAD1 C, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-
5、|1.65 0.04 0.35 0.02 0.09 ND1.77 0.02 392.79 287.18 99.91 252Integration Results for MSD1 TIC, MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.79 0.03 231554.91 106982.40 100.00 252MS Report from Instrument: LCMS-02LCMS-02 1/30/2018 16:25:09 XLH_854 Page 1 of 2Ret. Time: 1.79 m/z200 300 400 500 600 700 800 9000200040006000800010000ES-API Positive269.1140.1315.0159.1111.1253.1274.0252.1MS Report from Instrument: LCMS-02LCMS-02 1/30/2018 16:25:09 XLH_854 Page 2 of 2
