1、 File .8-3 2018-01-18 13-43-42CPK2018-117-08666.D Tgt Mass (CHM): Injection Date : 18 Jan 18 2:49 pm +0800 Seq. Line : 15Sample Name : CPK2018-117-08666 Location : P2-A-07Acq. Operator : HCL_771 Inj : 1Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:chem321DATA2018011820180118-3 201
2、8-01-18 13-43-421-POS-3MIN-1.MAnalysis Method : D:CHEM321DATA2018011820180118-3 2018-01-18 13-43-421-POS-3MIN-1.MCatalo No : HY-13785 Batch#08666 A-RP-189Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm
3、,3.5um A-RP-186Oven Temperature : 45Cmin0.5 1 1.5 2 2.5mAU010002000DAD1 B, Sig=214,4 Ref=off 0.4461.3051.5231.7791.8421.869min0.5 1 1.5 2 2.5mAU010002000DAD1 C, Sig=254,4 Ref=off 1.3041.4241.5221.8141.868min0.5 1 1.5 2 2.50200000400000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.334min0.5 1 1.5 2
4、2.50200004000060000Ion 334.7, MSD1 334.7,Target Mass 333.7 +H Positive, EIC=334.4:335.4 1.332Integration Results for DAD1 B, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|0.45 0.02 1.51 0.02 0.04 ND1.31 0.02 3491.83 2755.71 99.35 3341.52 0.03 16.44 17.62 0.47 3341.78 0.05 2.33 1.
5、93 0.07 3341.84 0.04 1.19 1.74 0.03 3341.87 0.06 1.42 1.82 0.04 334Integration Results for DAD1 C, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.30 0.02 3835.80 3198.33 99.63 3341.42 0.03 0.64 -0.02 0.02 3341.52 0.02 12.55 13.89 0.33 3341.81 0.05 0.48 0.02 0.01 3341.87 0.05 0.5
6、9 0.65 0.02 334Integration Results for MSD1 TIC, MS FileMS Report from Instrument: LCMS-02LCMS-02 1/18/2018 15:43:18 HCL_771 Page 1 of 3RetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.33 0.04 1534156.50 601226.00 100.00 334MS Report from Instrument: LCMS-02LCMS-02 1/18/2018 15:43:18 HCL_771 Page 2 of 3Ret. Time: 1.33 m/z200 300 400 500 600 700 800 900010000200003000040000500006000070000ES-API Positive337.0336.1334.0MS Report from Instrument: LCMS-02LCMS-02 1/18/2018 15:43:18 HCL_771 Page 3 of 3
